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专利名称:One pot diazotization, coupling and
quaternization of aminotriazoles
发明人:Hans-Peter Kuhlthau申请号:US06/2390申请日:19810223公开号:US04392998A公开日:19830712
摘要:In the preparation of a quaternized dyestuff of the formula ##STR1## in whichR.sup.1 and R.sup.2 each is an optionally substituted alkyl, alkenyl or aralkyl radical,
R.sup.3 is hydrogen, or an optionally substituted alkyl, aralkyl, cycloalkyl or arylradical, < P>< P> K is the radical of a coupling component+HK, and X is an anion,
< P> wherein an aminotriazole of the formula ##STR2## is diazotized and coupled toa coupling component HK to form an intermediate dyestuff of the formula ##STR3## andthe intermediate dyestuff is quaternized with an alkylating or aralkylating agent capableof providing the radicals R.sup.1 and R.sup.2 in a medium also providing the anion X.sup.-,the improvement which comprises effecting the coupling at a pH of 4 to 6 and thereafter,without isolation of the intermediate dyestuff, effecting the quaternization.
申请人:BAYER AKTIENGESELLSCHAFT
代理机构:Sprung, Horn, Kramer & Woods
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